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In another report, a microwave protocol was developed to reduce graphite oxide to graphene, which is used as a conductive additive in epoxy composites . The reduction of graphite oxide at the gram scale was performed in a microwave oven operated at 1,000 W of microwave power.

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Upon chemical oxidation of graphite to GO, it was observed that G band of GO goes broaden more than that of graphite and the intensity of D band of GO was increased over than D band of graphite, this can be explained by the decrease in size of the sp 2 carbon in crystalline domain by the creation of defects, vacancies, and distortions during oxidation [40,41].

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Also graphene and graphene oxide are used in cement composite pastes to enhance their mechanical and micro structural properties hence it was found that the addition of 0.03 wt% of GO can improve the mechanical strengths of cement composites by about 40%, while the incorporation of 0.05 wt% of GO into cement mortar enhanced the flexural strength by 70.5% as well as the compressive strength was …

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Synthesis of activated microwave exfoliated graphite oxide (aMEGO) The synthesis of porous graphene was achieved by the method previously described.20 It involved the following steps in sequence. (i) Preparation of GO (ii) microwave irradiation to prepare microwave exfoliated graphite oxide (MEGO), and (iii) activation of MEGO with potassium hydroxide.

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Graphene oxide is a unique material that can be viewed as a single monomolecular layer of graphite with various oxygen containing functionalities such as epoxide, carbonyl, carboxyl and hydroxyl groups.

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For the synthesis of graphite oxide, we used purified (99.9 wt.% C) graphite flakes of natural origin (codenamed as SGA-20) purchased from Kropfmühl GmbH, Germany. The samples were also fractionated by the manufacturer (d 90 < 50 µm, d 50 = 16–21 µm).

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